Books in the Chemical Analysis: A Series of Monographs on Analytical Chemistry and Its Applications series

Dealing with the principles of calibration--both the theoretical and mathematical constructs which relate features of calibration equations to the physical phenomena that affect instruments and samples used on generating information.

This monograph discusses fluorescence spectrometry, especially as applied to work in biochemistry, where the techniques are useful because of their high sensitivity and selectivity. The book also points out the utility of fluorescence when coupled to HPLC.

When bombarded with X-rays, solid materials produce distinct scattering patterns similar to fingerprints. X-ray powder diffraction is a technique used to fingerprint solid samples, which are then identified and cataloged for future use-much the way the FBI keeps fingerprints on file.

Describes the basic prerequisities for a fluorometric immunoassay: the antibody, the immunological technology, the fluorescent probe, and the instrument. Provides a profile of the clinical applications of the various assay technologies.

Polycyclic aromatic hydrocarbons (PAHs) were one of the first chemicals discovered to cause cancer in humans. This work covers polycyclic aromatic hydrocarbons with larger than seven rings. It has chapters devoted to sample handling and preparation and methodology.

Dealing with the various aspects of petroleum analysis, this book provides an explanation of the necessary standard tests that are applicable to feedstocks. The topics include: chemical composition; physical, thermal, electrical, and optical property testing methods; spectroscopic, chemical, and fractionation methods; molecular weight; and more.

X-ray fluorescence spectrometry (XRF) is a method of "fingerprinting" and identifying solid and liquid samples. Written by the leading international expert in the field, this totally-revised update provides an up-to-the-minute review of the progress of XRF in the last ten years, covering history, design, application, and interpretation.

This new edition includes: A chapter on the use of computer techniques in archaeological chemistry. A condensed introductory chapter, so that readers can get right into the "meat" of the book. Updated material on all the methods and techniques used to study the nature, age, and provenance of archaeological materials.

The authors are pioneering a new approach to classifying existing chemometric techniques for data analysis in one and two dimensions, using a practical applications approach to illustrating chemical examples and problems. Written in a simple, balanced, applications-based style, the book will appeal to both theorists and non-mathematicians.

This volume provides modern and practical analytical methodologies for the assays in foods, pharmaceuticals and clinical samples. Each chapter is written by experts in the particular area and includes original methods and the normal values which would be expected.

High performance capillary electrophoresis (HPCE) is a rapidly developing technology for separating and analyzing chemical compounds. The rapid developments in the field and the large number of journal publications have made it increasingly difficult to find essential and practical knowledge of HPCE easily.

This book concerns the design, operation and application of devices capable of generating acoustic waves in the ultrasonic frequency range. It emphasizes the study of chemical and/or biochemical systems imposed on the surface of such devices, whether operated in the gas- or liquid-phase, ie on acoustic wave chemical and biological sensors.

Graphite Furnace Atomic Absorption Spectrometry (GFAAS) is an established analytical laboratory technique used to examine materials in their vapor state by atomizing the sample in a graphite furnace. This approach is used mostly in the materials science and environmental analysis to examine alloys, polymers, ceramics, composites, and wastewater.

Presents an overview of applications, a critical evaluation of current techniques for sampling and for obtaining spectra, and an extensive guide to the literature, both spectra and papers. Covers everything from how to prepare almost any kind of sample and how to optimize the controls on an infrared spectrometer, to identifying and measuring pollutants at the parts per million level. Stresses all fundamental concepts and limitations; includes examples of difficulties and pitfalls throughout. Emphasizes development of technique and careful manipulation of samples and spectrometers. Highlights quantitative analysis with examples. Also reviews factors affecting group frequencies.

Illuminates emerging analytical techniques in high resolution mass spectrometry including time-of-flight mass spec. Provides a database of accurate masses for organic molecules, making o.m. detection much easier.

Principles and Practices of Polymer Mass Spectrometry helps readers acquire the skills necessary for selecting the optimal methods, handling samples, analyzing the data, and interpreting the results of the mass spectrometry of polymers. This guide describes the principles of polymer MS and best practices in polymer characterization.

Details methods for computing valid limits of detection.

Tandem Mass Spectrometry Edited by F.W. McLafferty More than 50 contributors, representing 32 of the world's leading research groups in mass spectrometry, examine the fundamentals, methods, instrumentation and applications of MS/MS, as well as promising new directions.

Identification of Microorganism by Mass Spectrometry teaches the reader how to use the latest techniques in mass spectrometry to identify the presence of microorganisms for biochemical, biomedical, pharmaceutical, and bioterror applications.

Describes various analytical techniques and systems for the development, validation, quality control, purification, and physicochemical testing of combinatorial libraries. This book provides coverage of applications of Nuclear Magnetic Resonance (NMR), liquid chromatography/mass spectrometry (LC/MS), and Fourier Transform Infrared (FTIR).

A timely, hands-on guide to environmental issues and regulatory standards for the petroleum industry Environmental analysis and testing methods are an integral part of any current and future refining activities. Today's petroleum refining industry must be prepared to meet a growing number of challenges, both environmental and regulatory.

Owing to its unique combination of high information content and ease of use, Raman spectroscopy, which uses different vibrational energy levels to excite molecules (as opposed to light spectra), has attracted much attention over the past fifteen years.

An invaluable reference tool for professional chemists and students of chemistry. While even the best analytical techniques cannot rectify problems generated by sloppy sample preparation, this less "sexy" step between the point at which analytes are transferred from the sample matrix to a form suitable for analysis is often overlooked.

This edition continues to provide analytical chemists and statisticians with the latest practical information on using statistical tools in chemical data analysis. The accompanying FTP site contains a series of programs that illustrate the statistical techniques which are discussed in the book.

A bestselling classic reference, now expanded and updated to cover the latest instrumentation, methods, and applications The Second Edition of Fourier Transform Infrared Spectrometry brings this core reference up to date on the uses of FT-IR spectrometers today.

In this revised and updated edition of his successful reference, Jungreis shares his expertise with readers to explore the contemporary utilization of simple spot and screening tests in clinical forensic, geochemical, and environmental applications.

The use of analytical methods in studies concerning works of art and archaeological artifacts provides essential information on the materials they are made from, including their composition, age, and methods used in their production. This book explains how to use analytical methods to obtain such information.

A definitive reference, completely updated Published in 1989, the First Edition of this book, originally entitled Quadrupole Storage Mass Spectrometry, quickly became the definitive reference in analytical laboratories worldwide.

Attenuated Total Reflection (ATR) spectroscopy is the most frequently used sampling technique for infrared spectroscopy, enabling samples to be examined in solid or liquid states. This book shows how ATR is used for materials that are either too thick or strong to be analyzed by other methods.

Provides a strong foundation in electrochemical principles and best practicesWritten for undergraduate majors in chemistry and chemical engineering, this book teaches the basic principles of electroanalytical chemistry and illustrates best practices through the use of case studies of organic reactions and catalysis using voltammetric methods and of the measurement of clinical and environmental analytes by potentiometric techniques. It provides insight beyond the field of analysis as students address problems arising in many areas of science and technology. The book also emphasizes electrochemical phenomena and conceptual models to help readers understand the influence of experimental conditions and the interpretation of results for common potentiometric and voltammetric methods.Electroanalytical Chemistry: Principles, Best Practices, and Case Studies begins by introducing some basic concepts in electrical phenomena. It then moves on to a chapter that examines the potentiometry of oxidation-reduction processes, followed by another on the potentiometry of ion selective electrodes. Other sections look at: applications of ion selective electrodes; controlled potential methods; case studies in controlled potential methods; and instrumentation. The book also features several appendixes covering: Ionic Strength, Activity and Activity Coefficients; The Nicolsky-Eisenman Equation; The Henderson Equation for Liquid Junction Potentials; Selected Standard Electrode Potentials; and The Nernst Equation Derivation.* Introduces the principles of modern electrochemical sensors and instrumental chemical analysis using potentiometric and voltammetric methods* Develops conceptual models underlying electrochemical phenomena and useful equations* Illustrates best practice with short case studies of organic reaction mechanisms using voltammetry and quantitative analysis with ion selective electrodes* Offers instructors the opportunity to select focus areas and tailor the book to their course by providing a collection of shorter texts, each dedicated to a single field* Intended as one of a series of modules for teaching undergraduate courses in instrumental chemical analysisElectroanalytical Chemistry: Principles, Best Practices, and Case Studies is an ideal textbook for undergraduate majors in chemistry and chemical engineering taking instrumental analysis courses. It would also benefit professional chemists who need an introduction to potentiometry or voltammetry.