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An increasingly popular analytical method, hydrophilic interaction chromatography (HILIC) has the ability to retain and separate polar compounds that are often difficult to analyze by reversed-phase high-performance liquid chromatography (HPLC) or other analytical methods.
This, the second part of a two-volume treatise, Inductively Coupled Plasma Emission Spectroscopy, addresses methodology, instrumentation and performance. Part 2 deals with applications and fundamentals.
Solid Phase Extraction (SPE) is a method of preparing samples for analysis. The technique involves purifying and concentrating a sample using a disposable column. This book explains how solid-phase extraction works and provides detailed applications of SPE in clinical, environmental, and natural product chemistry.
Recent developments in thin layer chromatography with important biochemical applications are presented in this text, which surveys recent trends and new equipment. Scanners designed to evaluate separations are described, including those for spectrocharacterization.
This volume discusses the impact of chirality and stereochemistry on drug development and use, including analytical, pharmacological and regulatory topics. It is wide-ranging and includes stereoisomeism in drug development.
This study demonstrates how the information theory approach to experimental data can be of benefit not only to analytical chemists but to all those using these techniques in the decision-making process. Emphasis is placed on the systems nature of analysis.
An invaluable reference tool for professional chemists and students of chemistry. While even the best analytical techniques cannot rectify problems generated by sloppy sample preparation, this less "sexy" step between the point at which analytes are transferred from the sample matrix to a form suitable for analysis is often overlooked.
Illuminates emerging analytical techniques in high resolution mass spectrometry including time-of-flight mass spec. Provides a database of accurate masses for organic molecules, making o.m. detection much easier.
Principles and Practices of Polymer Mass Spectrometry helps readers acquire the skills necessary for selecting the optimal methods, handling samples, analyzing the data, and interpreting the results of the mass spectrometry of polymers. This guide describes the principles of polymer MS and best practices in polymer characterization.
Dealing with the principles of calibration--both the theoretical and mathematical constructs which relate features of calibration equations to the physical phenomena that affect instruments and samples used on generating information.
Tandem Mass Spectrometry Edited by F.W. McLafferty More than 50 contributors, representing 32 of the world's leading research groups in mass spectrometry, examine the fundamentals, methods, instrumentation and applications of MS/MS, as well as promising new directions.
Identification of Microorganism by Mass Spectrometry teaches the reader how to use the latest techniques in mass spectrometry to identify the presence of microorganisms for biochemical, biomedical, pharmaceutical, and bioterror applications.
Describes various analytical techniques and systems for the development, validation, quality control, purification, and physicochemical testing of combinatorial libraries. This book provides coverage of applications of Nuclear Magnetic Resonance (NMR), liquid chromatography/mass spectrometry (LC/MS), and Fourier Transform Infrared (FTIR).
A timely, hands-on guide to environmental issues and regulatory standards for the petroleum industry Environmental analysis and testing methods are an integral part of any current and future refining activities. Today's petroleum refining industry must be prepared to meet a growing number of challenges, both environmental and regulatory.
Owing to its unique combination of high information content and ease of use, Raman spectroscopy, which uses different vibrational energy levels to excite molecules (as opposed to light spectra), has attracted much attention over the past fifteen years.
Presents an overview of applications, a critical evaluation of current techniques for sampling and for obtaining spectra, and an extensive guide to the literature, both spectra and papers. Covers everything from how to prepare almost any kind of sample and how to optimize the controls on an infrared spectrometer, to identifying and measuring pollutants at the parts per million level. Stresses all fundamental concepts and limitations; includes examples of difficulties and pitfalls throughout. Emphasizes development of technique and careful manipulation of samples and spectrometers. Highlights quantitative analysis with examples. Also reviews factors affecting group frequencies.
This edition continues to provide analytical chemists and statisticians with the latest practical information on using statistical tools in chemical data analysis. The accompanying FTP site contains a series of programs that illustrate the statistical techniques which are discussed in the book.
A bestselling classic reference, now expanded and updated to cover the latest instrumentation, methods, and applications The Second Edition of Fourier Transform Infrared Spectrometry brings this core reference up to date on the uses of FT-IR spectrometers today.
In this revised and updated edition of his successful reference, Jungreis shares his expertise with readers to explore the contemporary utilization of simple spot and screening tests in clinical forensic, geochemical, and environmental applications.
The use of analytical methods in studies concerning works of art and archaeological artifacts provides essential information on the materials they are made from, including their composition, age, and methods used in their production. This book explains how to use analytical methods to obtain such information.
A definitive reference, completely updated Published in 1989, the First Edition of this book, originally entitled Quadrupole Storage Mass Spectrometry, quickly became the definitive reference in analytical laboratories worldwide.
Attenuated Total Reflection (ATR) spectroscopy is the most frequently used sampling technique for infrared spectroscopy, enabling samples to be examined in solid or liquid states. This book shows how ATR is used for materials that are either too thick or strong to be analyzed by other methods.
Provides a strong foundation in electrochemical principles and best practicesWritten for undergraduate majors in chemistry and chemical engineering, this book teaches the basic principles of electroanalytical chemistry and illustrates best practices through the use of case studies of organic reactions and catalysis using voltammetric methods and of the measurement of clinical and environmental analytes by potentiometric techniques. It provides insight beyond the field of analysis as students address problems arising in many areas of science and technology. The book also emphasizes electrochemical phenomena and conceptual models to help readers understand the influence of experimental conditions and the interpretation of results for common potentiometric and voltammetric methods.Electroanalytical Chemistry: Principles, Best Practices, and Case Studies begins by introducing some basic concepts in electrical phenomena. It then moves on to a chapter that examines the potentiometry of oxidation-reduction processes, followed by another on the potentiometry of ion selective electrodes. Other sections look at: applications of ion selective electrodes; controlled potential methods; case studies in controlled potential methods; and instrumentation. The book also features several appendixes covering: Ionic Strength, Activity and Activity Coefficients; The Nicolsky-Eisenman Equation; The Henderson Equation for Liquid Junction Potentials; Selected Standard Electrode Potentials; and The Nernst Equation Derivation.* Introduces the principles of modern electrochemical sensors and instrumental chemical analysis using potentiometric and voltammetric methods* Develops conceptual models underlying electrochemical phenomena and useful equations* Illustrates best practice with short case studies of organic reaction mechanisms using voltammetry and quantitative analysis with ion selective electrodes* Offers instructors the opportunity to select focus areas and tailor the book to their course by providing a collection of shorter texts, each dedicated to a single field* Intended as one of a series of modules for teaching undergraduate courses in instrumental chemical analysisElectroanalytical Chemistry: Principles, Best Practices, and Case Studies is an ideal textbook for undergraduate majors in chemistry and chemical engineering taking instrumental analysis courses. It would also benefit professional chemists who need an introduction to potentiometry or voltammetry.
An overview of current research and developments in ultrasensitive bioanalysis New platforms of ultrasensitive analysis of biomolecules and single living cells using multiplexing, single nanoparticle sensing, nano-fluidics, and single-molecule detection are advancing every scientific discipline at an unprecedented pace.
Dealing with the various aspects of petroleum analysis, this book provides an explanation of the necessary standard tests that are applicable to feedstocks. The topics include: chemical composition; physical, thermal, electrical, and optical property testing methods; spectroscopic, chemical, and fractionation methods; molecular weight; and more.
Focusing on the technology of optimum data acquisition, this text presents coverage of the development of Fourier transform instruments and their application to problems in planetary and Earth atmospheric research. There is also a summary of the sampling and data processing aspects.
A sensor is an extremely sensitive measuring device. The measuring can be conducted by chemical, mechanical, biological, optic, or electronic means. Sensors are encountered everyday, be it the bomb detector in an airport, the gas gauge of an automobile, or the smoke detector in the home.
High-Resolution Solid-State NMR of Silicates and Zeolites Gunter Engelhardt and Dieter Michel "I strongly recommend this book as an important reference for scientists concerned with the structural properties of siliceous materials.
This volume is concerned with the application of fluorescence, phosphorescence and chemiluminescence spectra to the analysis of organic and inorganic compounds. It also deals with the use of these spectra to extract data about the structure and function of biological macromolecules.
For the analyses of DNA and RNA, high pressure/performance liquid chromatography has proven itself to be extremely useful. This text deals with both trace and ultratrace analyses at or below ppm level. A variety of applications and methods are discussed, as well as equipment considerations.
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